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VRSTA GRADIVAanalitična raven (sestavni del), tekstovno gradivo, tiskano, 1.01 - izvirni znanstveni članek
DRŽAVA IZIDASlovenija
LETO IZIDA2007
JEZIK BESEDILA/IZVIRNIKAangleški
PISAVAlatinica
ODGOVORNOSTButinar, Bojan - avtor // Bučar-Miklavčič, Milena - avtor // Bešter, Erika - avtor // Valenčič, Vasilij - avtor
NASLOVEvaluation of measurement uncertainty for the methods of analysis used to assess the characteristics of olive oil and olive-pomace oil from commission regulations EEC 2568/91 and EC 1989/2003 -a case sample evaluating the measurement uncertainty for peroxide value = Valutazione dell'incertezza di misura di metodi di analisi usati per accertarele caratteristiche degli oli d'oliva e degli oli di sansa d'oliva secondo i regolamenti cee 2568/91 ed ce 1989/2003 - esempio di valutazione dell'incertezza di misura per dell'indice di perossido
V PUBLIKACIJIAnnales. Series historia naturalis. - ISSN 1408-533X. - ǂLetn. ǂ17, ǂšt. ǂ1 (2007), str. 123-132.
KRATKA VSEBINAMetrology has been present in our scientific knowledge for a long time, but mostly in physical measurements. Chemical measurement can be defined as a comparison of a quantity of measurand and relating it to a unit (e.g. mol/kg).When expressing a result of a measurement, the problem of traceability, validation and the measurement uncertainty (MU) evaluation must be challenged. It is well known that MU isa parameter associated with the result of a measurement that characterizes the dispersion of the values that could reasonably be attributed to the measurand. The EEC document 2568/91 with its annexes gives the methods of analysis to assess the characteristics of olive oils and olive-pomace oils with given limits. The EC document 1989/2003 gives the scheme, the algorithm, the pathway, the decision tree to differentiate between various types of olive oils using the particular determinations based on limits. The major lack of these EC methods is the non-existence of validation parameters, which are crucial in determining the MU (and in accreditation of a laboratory). There are several ways of evaluating (better term than calculating) the MU: with model equation, with use of a certified referencematerial (CRM) and with participation in a proficiency testing (PT) scheme.MU for a method of analysis is inherent to a laboratory and can serve as a tool for 'measuring' the quality of a laboratory. Unfortunately, there are practically no CRM's in the olive oil testing field. The only way to achieve a usable MU is through participation in PT schemes.
OPOMBEBesedilo v angl. // Bibliografija: str. 132 //Abstract ; Sintesi ; Povzetek
OSTALI NASLOVIOvrednotenje merilne negotovosti analiznih metod za ugotavljanje značilnosti oljčnega olja in olja iz oljčnih tropin iz uredb EGS 2568/91 in ES 1989/2003 -primer ovrednotenja merilne negotovosti peroksidnega števila
PREDMETNE OZNAKE// meroslovje // metrologija // oljčno olje // kemijska analiza // negotovost // peroksidno število
UDK006.91, 665.327.3:543

izvedba, lastnina in pravice: NUK 2010